Wednesday, October 28, 2009 8:30 Registration 9:30 Meeting Start Carmen Dorronsoro and Joan O. Grimalt University of the Basque Country and Institute of Environmental Assessment and Water Research (IDÆA-CSIC) Plenary session Chairman. Emilio Gelpi Institute of Biomedical Research of Barcelona (IIBB-CSIC) 10:0 Invited lecture: Illicit drugs in water resources. From wastewater to tap water Maria Teresa Galceran Faculty of Chemistry. University of Barcelona 11:00 Coffee 11:30 Invited lecture: Tracing drugs of abuse in waste waters, natural waters and airborne particles at the Ebro River Basin, Barcelona and Madrid metropolitan areas Damià Barceló Institute of Environmental Assessment and Water Research (IDÆA-CSIC) Oral communications Room A Chairman. Francisco Javier Santos University of Barcelona 12:30 – 12:50 Can drugs of abuse reach Spanish tap waters? M.R. Boleda1, M. Huerta-Fontela1, M.T. Galceran2, F. Ventura1
1AGBAR. Aigües de Barcelona. 2Department of Analytical Chemistry, University of Barcelona. 12:50 – 13:10 Illicit drugs through water treatment: generation of new disinfection-by-products M. Huerta-Fontela1, M.T. Galceran2, F. Ventura1
1AGBAR-Aigües de Barcelona. 2Department of Analytical Chemistry, University of Barcelona. 13:10 – 13:30 Screening for anabolic steroids, β2-agonists, corticosteroids, and other compounds of doping interest by ultraperformance liquid chromatography-tandem mass spectrometry R. Ventura1,2,, M. Roig1,2, N. Monfort1,2, P. Saez1, C. Gómez1,2, R. Bergés1, J. Segura1,2
1Grup de Recerca em Bioanàlisi , IMIM-Hospital del Mar, Barcelona. 2Departament de Ciències Experimentals i de la Salut, Universitat Pompeu Fabra, UPF, Barcelona. 13:30 – 13:50 Analysis and monitoring of illegal or misused pesticides in european and imported fruits and vegetables A.R. Fernandez-Alba, O. Malato, M. Mezcua, A. Agüera. Pesticide Residue Research Group. EU Community Reference Laboratory University of Almeria.
13:50 – 14:10 Presence of sildenafil, vardenafil and tadalafil in influent and effluent wastewater and sewage sludge A. Nieto1,2, M. Peschka1, F. Borrull2, E. Pocurull2, R.M. Marcé2, T.P. Knepper1
1 University of Applied Sciences Fresenius. Idstein, Germany. 2 Department of Analytical Chemistry and Organic Chemistry, Faculty of Chemistry, University Rovira i Virgili. Tarragona. Room B Chairman. Juan Manuel Madariaga University of the Basque Country 12:30 – 12:50 Optimisation of membrane-assisted solvent extraction (MASE) for the determination of several endocrine disruptor compounds in water samples R. Rodil1, A. Vallejo1, A. Prieto1, O. Basauri2, A. Usobiaga2, N. Etxebarria2, L.A. Fernández2, O. Zuloaga2
1Department ofAnalytical Chemistry, Nutrition and Food Sciences, IIAA - Institute for Food Analysis and Research, University of Santiago de Compostela. 2Department of Analytical Chemistry, Faculty of Science and Technology, University of Basque Country. Leioa. 12:50 – 13:10 The next stage in mixed-mode technology: ion-exchange hypercrosslinked sorbents to selective extract pharmaceuticals in complex environmental samples N. Fontanals, D. Bratkowska, P.A.G. Cormack, D.C. Sherrington, R.M. Marcé, F. Borrull Department of Analytical Chemistry and Organic Chemistry, Faculty of Chemistry, University Rovira i Virgili. Tarragona. 13:10 – 13:30 Selective pressurised liquid extraction of polychlorinated biphenyls from sediments M. Pena-Abaurrea, J.J Ramos, M.J. González and L. Ramos Department of Instrumental Analysis and Environmental Chemistry, Institute of Organic Chemistry, IQOG-CSIC. Madrid 13:30 – 13:50 Extraction of pesticides from bananas, grapes and plums using ionic liquid based dispersive liquid-liquid microextraction J. Hernández-Borges, L.M. Ravelo-Pérez, T.M. Borges-Miquel, M.A. Rodríguez-Delgado Departamento de Química Analítica, Nutrición y Bromatología, Facultad de Química, Universidad de La Laguna (ULL). 13:50 – 14:10 On-line versus off-line solid-phase extraction for the determination of microcystins in waters by ultra fast liquid chromatography coupled to tandem mass spectrometry M. Huerta-Fontela1, M. Sibum2, F. Ventura1
1AGBAR-Aigües de Barcelona. 2Spark Holland: Emmen (The Netherlands) 14:10 Lunch 15:00 Poster session 15:00 Workshop of Thermo Fisher Scientific
Analysis of antibiotics in complex food matrices (Turboflow-LC-TQ-MS/MS) C. Martins, S. Guazzotti Termo Fisher Scientific 17:00 Coffee Oral communications Room A Chairman. Lourdes Cantón University of the Basque Country 17:30-17:50 Determination of phytoestrogens in beer by high performance liquid chromatography with diode array detection J. Bernal1. C. Martinez García-Mauriño1, F.R. Marin2, G. Reglero2, A. Cifuentes1, E. Ibañez1
1Institute of Industrial Fermentations (CSIC). Madrid. 2Sección Departamental Ciencias de la Alimentación, Universidad Autónoma de Madrid. 17:50-18:10 High temperature liquid chromatography coupled to inductively coupled plasma atomic emission spectrometry. application to the analysis of foods A. Terol, E. Paredes, S. E. Maestre, M.S. Prats, J.L. Todolí Department of Analytical Chemistry, Nutrition and Food Sciences, Faculty of Sciences, University of Alicante. 18:30-18:50 Confirmatory method to determine antimicrobials in chicken by QuEChERs and liquid chromatography tandem mass spectrometry C. Blasco1, A. Masia1, F. Morillas2, Y. Picó1
1Área de Nutrició i Bromatologia, Facultat de Farmàcia, Universitat de València. 2Departament d'Economia Aplicada, Facultat d'Economia Universitat de València. Room B Chairman. Begoña Jimenez University of Barcelona 17:30-17:50 Development of a microdevice system for microchip electrophoretical separations with fluorescent detection. application to milk proteins analysis. M.M. Barrios-Romero, A. González-Crevillén, J. Otero-Robledo, M. de Frutos, J.C. Diez-Masa Institute of Organic Chemistry (C.S.I.C.). Madrid. 17:50-18:10 Expanding de triple quadrupole portfolio of Agilent technologies. The right system for the right application J. Aybar Life Sciences and Chemical Analysis, Agilent Technologies. Las Rozas de Madrid. 18:30-18:50 Challenges in HPLC: more efficiency, more ruggedness, more sensibility and … Ascentis Express Denise Wallworth Sales Development Manager. HPLC. Sigma Aldrich
18:50-19:10 Validation of an HPLC-FLD analytical method for the detection of aflatoxin B1 and ochratoxin a in rat plasma, liver and kidney. LA. Corcuera1, M. Ibáñez-Vea2, A. Vettorazzi1, E. González-Peñas2, A. López de Cerain1
1Nutrition and Food Sciences, Physiology and Toxicology Department. Faculty of Pharmacy. University of Navarra. 2Organic and Pharmaceutical Chemistry Department. Faculty of Pharmacy. University of Navarra. 19:10 End 20:00 Reception in the Donostia-San Sebastian City Hall
Thursday, October 29, 2009 Plenary session Chairman. Rosa Maria Marcè University Rovira i Virgili. Tarragona. 9:00 Invited lecture: Selective sample preparation for LC-MS(/MS) analysis of biologically active compounds combining chemical and biological information Henk Lingeman and Hubertus Irth Free University of Amsterdam. Amsterdam. The Netherlands Oral communications Room A Chairman. Pilar Fernandez Institute of Environmental Assessment and Water Research (IDÆA-CSIC) 10:00-10:20 Emerging pollutants in protected natural areas P. Vazquez-Roig1, C. Blasco1, V. Andreu2, Y. Picó1
1Departament of toxicology. Faculty of Pharmacy, University of Valencia. 2Centro de Investigaciones sobre Desertificación–CIDE. Albal, València. 10:20-10:40 Multiresidue analysis of POPs in fish products from the Ebro River Delta (Catalonia, Spain) M. Ábalos1, J. Parera1, M.G. Martrat1, F.J. Santos2, X. Llebaria3, M.T. Galceran2, J. Rivera1, E. Abad1
1Dioxin Lab., Environmental Chemistry Dept., IDÆA-CSIC. Barcelona. 2Analytical Chemistry. Dept., U. Barcelona. 3Health Dept., Generalitat de Catalunya. Barcelona. 10:40-11:00 Comparison of determination methods for pesticide residue analysis: use of quadrupole time-of-flight in liquid chromatography Y. Picó1, M. Farré2, C. Blasco1, D. Barceló2,3
1Laboratori de Nutrició i Bromatologia, Facultat de Farmàcia, Universitat de València. Burjassot, Valencia. 2Department of Environmental Chemistry, IDÆA-CSIC. Barcelona. 3Catalan Institute of Water Research, ICRA. Girona
Room B Chairman. Ana Agüera University of Almería 10:00-10:20 Two-dimensional liquid-chromatographic separations hyphenated to Q-TOF spectrometry for urinary metabolomic fingerprinting A.L. Huidobro, C. Barbas Sección de Química Analítica. Facultad de Farmacia. Universidad San Pablo-CEU. Boadilla del Monte. Madrid. 10:20-10:40 Modelling of gas chromatographic response for its estimation in comprehensive two-dimensional gas chromatography (GC×GC) M. Brok1, M.L. Sanz1, A.C. Soria2, J. Sanz1
1Instituto de Química Orgánica General (CSIC), 2Instituto de Fermentaciones Industriales (CSIC).Madrid. 10:40-11:00 DDT occurrence and origin in the surroundings of Doñana National Park. Application of monodimensional and heart-cutting multidimensional chromatography. J. Muñoz-Arnanz, B. Jiménez Department of Instrumental Analysis and Environmental Chemistry, Institute of Organic Chemistry, (CSIC). Madrid. 11:00 Coffee Plenary Session Chairman. Xavier Guardino Centro Nacional de Condiciones de Trabajo. INSHT. Barcelona 11:30 Invited lecture: Monolithic silicas in High-Performance Liquid Chromatography (HPLC) - where is the added value as compared to particle packed columns? Klaus K. Unger, R. Ditz, E. Machtejevas and R. Skudas Institut für Anorganische Chemie und Analytische Chemie. Johannes Gutenberg-Universität. Mainz. Germany 12:30 Session of poster discussion Room A. Environment Chairmen. Pilar Fernandez and Jesús Ibarluzea Institute of Environmental Assessment and Water Research (IDÆA-CSIC) and University of the Basque Country Room B. Food and food safety Chairmen. Elena Ibáñez and Yolanda Picó Institute of Industrial Fermentations (IFI-CSIC) and University of Valencia 14:00 Lunch 15:00 Poster session 15:00 Workshop of Agilent
Metabolomics, a new approach to bioanalysis with separation techniques and mass spectrometry C. Barbas1, A. García1, I. García-Pérez1, S. Angulo1, J. Teul2, M. Ciborowski2, M.P. Martínez-Alcázar1, J. Rupérez1
1CEMBIO. Facultad de Farmacia. Universidad San Pablo-CEU. Boadilla del Monte. Madrid. 2Medical University of Bialystok. Bialystok (Poland) 17:00 Coffee 17:15 General Assembly of SECyTA 21:00 Meeting Dinner at the Miramar Palace
Friday, October 30, 2009 Plenary session Chairman. Carmen Dorronsoro University of the Basque Country 9:30 Invited lecture: Analytical strategies based on triple quadrupole and time-of- flight LC-MS for the determination of pesticide residues Félix Hernández Faculty of Sciences. University Jaume I. Castelló de la Plana 10:30 Poster session Room A. Bioanalysis. Clinical analysis Chairmen. Ana García Campaña and Emilio Gelpí University of Granada and Institute of Biomedical Research of Barcelona (IIBB-CSIC) Room B. New developments. Other Chairmen. Begoña Jiménez and Francisco Javier Santos Institute of General Organic Chemistry (IQOG-CSIC) and University of Barcelona 12:00 Coffee Oral communications Room A Chairman. Yolanda Pico University of Valencia 12:30-12:50 Accurate quantitation of melon aroma components using multiple- headspace-solid phase microextraction followed by gas chromatography-mass spectrometry E. Serrano, J. Beltrán, F. Hernández Research Institute for Pesticides and Water, Jaume I University. Castellón, Spain
12:50-13:10 Trace determination of chlorophenols and other chlorinated pesticides in several concentration ranges by SPME-GC/ECD F.J. Yuste-Córdoba, A.B. Botet-Jiménez, D. Omenat-Morán Grupo de Investigación “Química Medioambiental y Sostenible”, Departamento de Tecnología y Calidad. Instituto del Corcho, la Madera y el Carbón Vegetal. Mérida (Badajoz). 13:10-13:30 Retention-liberation studies of penconazole applied as topas formulation in vineyard soils E. Pose-Juan1,2, R. Rial-Otero1, E. López-Periago2, M. Paradelo2, J. Simal-Gándara1
1Analytical and Food Chemistry Department. 2Plant Biology and Soil Science Department. Faculty of Science of Ourense, University of Vigo. 13:30-13:50 Preparation of a sewage sludge reference material for the determination of alkylphenols and alkylphenols ethoxylates M. Fernández1, A. Rigol1, A. Sahuquillo1, S. Lacorte2
1Departament de Química Analítica. Universitat de Barcelona. 2Departament of Environmental Chemistry, (IDAEA-CSIC). Barcelona. Room B Chairman. Elena Ibáñez Institute of Industrial Fermentations (IFI-CSIC) 12:30-12:50 Analysis of linear and cyclic siloxanes in sewage sludge by concurrent solvent recondensation –large volume injection-GC-MS E.Y. Companioni, F.J. Santos, M.T. Galceran. Department of Analytical Chemistry. Chemistry Faculty. University of Barcelona. 12:50-13:10 Quantitative structure–retention relationships modelling of retention indices on poly(3,3,3-trifluoropropylmethyl siloxane) stationary phases P. Galindo-Iranzo1, R. Lebrón-Aguilar1, J.E. Quintanilla-López1,2
1Instituto de Química-Física “Rocasolano” (CSIC). Madrid. 2Dpto. Ingeniería Química Industrial y del Medio Ambiente, ETSI Industriales (UPM). Madrid 13:10-13:30 Characterization of O-sialoglycopeptides from hydrolyzed caseinomacropeptide using hydrophilic interaction liquid chromatography (HILIC) tandem mass spectrometry O. Hernández1, R. Lebrón-Aguilar2, J.E. Quintanilla-López2,3, M.L. Sanz1, F.J. Moreno4
1Instituto de Química Orgánica General (CSIC). Madrid. 2Instituto de Química-Física “Rocasolano” (CSIC). Madrid. 3Departamento de Ingeniería Química Industrial y del Medio Ambiente, ETS Ingenieros Industriales (UPM). Madrid. 4Instituto de Fermentaciones Industriales (CSIC). Madrid. 13:30-13:50 Comparison of different advanced extraction techniques to obtain polyphenolic antioxidants from rosemary (Rosmarinus officinalis). M. Herrero1,2, M. Plaza1, A. Cifuentes1, E. Ibáñez1
1Departamento de Caracterización de Alimentos, Instituto de Fermentaciones Industriales (CSIC). Madrid. 2Sección Departamental de Ciencias de la Alimentación. Universidad Autónoma de Madrid. 13:50-14:10 Identification of the biotransformation products of 2-ethylhexyl 4-(N,N-dimethylamino) benzoate. an analytical method for their determination in human urine Z. León1, J. de Vlieger2, A. Chisvert1, A. Salvador1, H. Lingeman2, H. Irth2, M. Giera2
1Departamento Química Analítica, Facultad Química, Universitat de València. 2Department of Chemistry. BioMolecular Analysis Group. Faculty of Sciences. VU University Amsterdam. The Netherlands 14:10 Awards ceremony and end of Meeting 14.45 Farewell cocktail
Le elezioni europee in Polonia e in Repubblica ceca di Simona Guerra (Università di Nottingham) Introduzione Le precedenti elezioni europee del 2004 hanno registrato una bassa affluenza record nei nuovi Stati membri dell’Europa centro-orientale e delineato una spaccatura profonda con i Paesi dell’Europa occidentale. Il 55.63 per cento dei cittadini ha votato nei ‘vecchi’ Paesi
Seelsorge für die Industrie Die Elite der Nervenheilkunde ist eng mit Pharmakonzernen verflochten: Psychiater, Neurologen, aber auch Psychologen arbeiten als bezahlte Berater für die Unternehmen. Nun fordert ein Professor seine Kollegen auf, ihre Nebeneinkünfte offenzulegen. Wer den Nervenarzt Matthias Riepe fragt, ob er Geld von Pharmafirmen annehme, erlebt ein kurzes Gespräch. "